File 1 : H:\instruments-archive\XRD-current\Austin\MCTeCO\ML_McNulty_20240116_4_AMF-RbCTeCO_T7_dried+Si_std_2hr_last_check.raw Range Number : 1 R-Values Rexp : 1.09 Rwp : 1.79 Rp : 1.29 GOF : 1.65 Rexp`: 6.97 Rwp`: 11.47 Rp` : 14.55 DW : 0.83 Quantitative Analysis - Rietveld Phase 1 : Structure 92.65(18) % Phase 2 : Structure 7.35(18) % Background Chebychev polynomial, Coefficient 0 7896(4) 1 -3607(7) 2 609(6) 3 206(6) 4 126(6) 5 -431(6) 6 329(6) 7 -67(5) 8 -87(5) 9 58(5) 10 6(5) Instrument Primary radius (mm) 200.5 Secondary radius (mm) 200.5 Linear PSD 2Th angular range (°) 3 FDS angle (°) 0.6 Corrections Specimen displacement 0.121(6) LP Factor 0 Miscellaneous Convolution Steps 3 Start X 12 Finish X 60 Structure 1 Phase name Structure R-Bragg 0.514 Spacegroup C2/c Scale 0.000189(3) Cell Mass 2467(3) Cell Volume (Å^3) 757.30(4) Wt% - Rietveld 92.65(18) Double-Voigt|Approach Cry size Lorentzian 84.2(19) k: 1 LVol-IB (nm) 54(2) k: 0.89 LVol-FWHM (nm) 75(3) Strain Strain L 0.048(8) e0 0.00010(11) Crystal Linear Absorption Coeff. (1/cm) 1217.43(8) Crystal Density (g/cm^3) 5.410(7) Preferred Orientation Spherical Harmonics Order 4 y00 1 y20 -0.334(18) y22m -0.91(3) y22p 0.111(5) y40 -0.069(13) y42m 0.006(15) y42p 0.058(5) y44m -0.108(8) y44p -0.492(17) Lattice parameters a (Å) 12.6727(4) b (Å) 5.20635(18) c (Å) 11.6213(4) beta (°) 99.008(3) Site Np x y z Atom Occ Beq Co1 8 0.2715(5) 0.3112(16) 0.1497(6) Co 0.955(9) 1.4(3) Te1 4 0.50000 0.6534(7) 0.25000 Te 1.000(7) 0.88(18) Te2 8 0.3622(2) 0.3082(5) 0.4442(3) Te 0.990(8) 1.29(15) O1 8 0.4169(17) 0.453(5) 0.159(2) O 0.92(2) 2.0(9) O2 8 0.3756(18) 0.601(4) 0.360(2) O 1.00(3) 1.0(8) O3 8 0.2925(16) 0.148(5) 0.320(2) O 0.97(3) 1.0(8) O4 8 0.254(2) 0.437(4) 0.470(2) O 0.99(2) 2.0(9) Structure 2 Phase name Structure R-Bragg 0.496 Spacegroup Fd-3m Scale 0.000779(17) Cell Mass 224.684 Cell Volume (Å^3) 160.14989 Wt% - Rietveld 7.35(18) Double-Voigt|Approach Cry size Gaussian 310(50) k: 1 LVol-IB (nm) 290(60) k: 0.89 LVol-FWHM (nm) 270(50) Crystal Linear Absorption Coeff. (1/cm) 148.024 Crystal Density (g/cm^3) 2.330 Preferred Orientation Spherical Harmonics Order 4 k00 1 k41 -1.17(7) Lattice parameters a (Å) 5.4305300 Site Np x y z Atom Occ Beq Si1 8 0.00000 0.00000 0.00000 Si 1 0.54