File 1 : H:\instruments-archive\XRD-current\Austin\MCTeCO\ML_Westley_20240202_1_AMF-LiCTeCO_T8_dried+Si_std_2hr_last_check.raw Range Number : 1 R-Values Rexp : 1.12 Rwp : 2.39 Rp : 1.47 GOF : 2.13 Rexp`: 7.30 Rwp`: 15.57 Rp` : 18.97 DW : 0.72 Quantitative Analysis - Rietveld Phase 1 : Structure 65.7(2) % Phase 2 : Structure 34.3(2) % Background Chebychev polynomial, Coefficient 0 7491(5) 1 -3841(9) 2 461(8) 3 440(7) 4 74(7) 5 -543(7) 6 418(7) 7 -114(6) 8 -97(6) Instrument Primary radius (mm) 200.5 Secondary radius (mm) 200.5 Linear PSD 2Th angular range (°) 3 FDS angle (°) 0.6 Corrections Specimen displacement 0.106(2) LP Factor 0 Miscellaneous Convolution Steps 3 Start X 12 Finish X 60 Structure 1 Phase name Structure R-Bragg 0.717 Spacegroup C2/c Scale 0.000100(4) Cell Mass 2473(4) Cell Volume (Å^3) 758.57(6) Wt% - Rietveld 65.7(2) Double-Voigt|Approach Cry size Lorentzian 116.4(17) k: 1 LVol-IB (nm) 74.1(11) k: 0.89 LVol-FWHM (nm) 103.6(15) Strain Strain L 0.048(6) e0 0.000104(12) Crystal Linear Absorption Coeff. (1/cm) 1225.08(11) Crystal Density (g/cm^3) 5.413(10) Preferred Orientation Spherical Harmonics Order 4 y00 1 y20 0.13(2) y22m -0.27(2) y22p 0.147(12) y40 -0.23(2) y42m -0.24(3) y42p 0.047(11) y44m -0.127(16) y44p -0.119(15) Lattice parameters a (Å) 12.6818(6) b (Å) 5.2091(2) c (Å) 11.6257(5) beta (°) 98.987(4) Site Np x y z Atom Occ Beq Co1 8 0.2746(9) 0.312(3) 0.1439(10) Co 0.972(11) 1.8(4) Te1 4 0.50000 0.6522(13) 0.25000 Te 1.000(10) 1.5(3) Te2 8 0.3610(4) 0.3085(9) 0.4443(6) Te 0.997(12) 2.4(2) O1 8 0.421(3) 0.447(7) 0.150(4) O 0.94(3) 3.0(14) O2 8 0.367(3) 0.610(8) 0.353(5) O 1.00(4) 3.0(14) O3 8 0.289(3) 0.141(10) 0.328(4) O 0.87(4) 1.6(14) O4 8 0.251(4) 0.463(8) 0.477(5) O 0.98(3) 2.9(14) Structure 2 Phase name Structure R-Bragg 1.787 Spacegroup Fd-3m Scale 0.00272(3) Cell Mass 224.684 Cell Volume (Å^3) 160.14989 Wt% - Rietveld 34.3(2) Double-Voigt|Approach Cry size Lorentzian 400(30) Cry size Gaussian 253(10) k: 1 LVol-IB (nm) 142(5) k: 0.89 LVol-FWHM (nm) 162(5) Strain Strain G 0.034(12) e0 0.00007(3) Crystal Linear Absorption Coeff. (1/cm) 148.024 Crystal Density (g/cm^3) 2.330 Preferred Orientation Spherical Harmonics Order 4 k00 1 k41 -0.66(3) Lattice parameters a (Å) 5.4305300 Site Np x y z Atom Occ Beq Si1 8 0.00000 0.00000 0.00000 Si 1 0.54