File 1 : H:\instruments-archive\XRD-current\Austin\MCTeCO\ML_McNulty_20240116_3_AMF-KCTeCO_T81_dried+Si_std_2hr_last_check.raw Range Number : 1 R-Values Rexp : 1.11 Rwp : 2.41 Rp : 1.55 GOF : 2.17 Rexp`: 6.07 Rwp`: 13.17 Rp` : 15.87 DW : 0.87 Quantitative Analysis - Rietveld Phase 1 : Structure 65.9(5) % Phase 2 : Structure 34.1(5) % Background Chebychev polynomial, Coefficient 0 7492(5) 1 -3165(8) 2 495(8) 3 213(8) 4 171(7) 5 -497(7) 6 353(7) 7 -75(6) 8 -83(6) Instrument Primary radius (mm) 200.5 Secondary radius (mm) 200.5 Linear PSD 2Th angular range (°) 3 FDS angle (°) 0.6 Corrections Specimen displacement 0.044(2) LP Factor 0 Miscellaneous Convolution Steps 3 Start X 12 Finish X 60 Structure 1 Phase name Structure R-Bragg 0.649 Spacegroup C2/c Scale 0.000156(3) Cell Mass 2477(4) Cell Volume (Å^3) 758.02(4) Wt% - Rietveld 65.9(5) Double-Voigt|Approach Cry size Lorentzian 113.1(14) k: 1 LVol-IB (nm) 72.0(9) k: 0.89 LVol-FWHM (nm) 100.6(12) Crystal Linear Absorption Coeff. (1/cm) 1225.03(9) Crystal Density (g/cm^3) 5.427(8) Preferred Orientation Spherical Harmonics Order 4 y00 1 y20 -0.20(3) y22m -0.67(4) y22p 0.086(8) y40 -0.073(19) y42m -0.05(2) y42p 0.053(7) y44m -0.059(11) y44p -0.37(3) Lattice parameters a (Å) 12.6780(4) b (Å) 5.20807(14) c (Å) 11.6236(3) beta (°) 99.006(2) Site Np x y z Atom Occ Beq Co1 8 0.2704(6) 0.3078(18) 0.1478(7) Co 0.980(11) 1.3(3) Te1 4 0.50000 0.6526(8) 0.25000 Te 1.000(8) 1.1(2) Te2 8 0.3625(3) 0.3087(6) 0.4435(4) Te 0.991(9) 1.55(18) O1 8 0.419(2) 0.449(6) 0.148(3) O 0.94(2) 1.2(10) O2 8 0.377(2) 0.612(5) 0.360(3) O 1.00(3) 0.9(10) O3 8 0.2954(19) 0.144(6) 0.318(3) O 0.94(3) 1.6(10) O4 8 0.249(2) 0.458(5) 0.473(3) O 0.97(3) 2.0(11) Structure 2 Phase name Structure R-Bragg 1.027 Spacegroup Fd-3m Scale 0.00421(4) Cell Mass 224.684 Cell Volume (Å^3) 160.14989 Wt% - Rietveld 34.1(5) Double-Voigt|Approach Cry size Lorentzian 1100(200) Cry size Gaussian 350(30) k: 1 LVol-IB (nm) 250(20) k: 0.89 LVol-FWHM (nm) 260(20) Crystal Linear Absorption Coeff. (1/cm) 148.024 Crystal Density (g/cm^3) 2.330 Preferred Orientation Spherical Harmonics Order 4 k00 1 k41 -0.14(2) Lattice parameters a (Å) 5.4305300 Site Np x y z Atom Occ Beq Si1 8 0.00000 0.00000 0.00000 Si 1 2.9(5)